LOW TEMPERATURE RESEARCH FACILITY
Resistivity, Magneto-resistance, and Hall Effect
Electrical transport measurements on materials are carried out as a function
of temperature. This system makes use of a liquid helium cryostat that houses
a 10 Tesla superconducting magnet. The temperature of a sample may be varied
from 2 K to 300 K and can be held constant with an accuracy of +/- 0.05K.
The collection of data and the regulation of sample temperature is computer
controlled. Design and construction of much of this system was carried out by
undergraduate physics majors at Brockport. A detailed discussion of this
system was publushed in the Proceedings of the National Conference on
Undergraduate Research. See the He4 cryostat (1.2K < T < 300K), with insert being leak tested.
A.C. Magnetic Susceptibility
Materials ac magnetic susceptibility is studied/measured using a Hartshorn
Bridge as modified by Maxwell, and an SAR850 Lock-in-Detector in the same
temperature range. In collaboration with D. I. Popov, the magnetic susceptibility
and the resistivity have actually been measured simultaneously on the same sample
on indium doped tin-lead telluride semiconducting samples with superconducting
properties below 4.2 K, with obvious correlation, but not so obvious results.
D.C. Magnetic Susceptibility
Magnetization is measured using an Oxford Instruments RF SQUID magnetometer
with a temperature range extanded down to 0.33K, using a Janis He3
refrigerator.
R. V. Mancuso and MZT are collaborating on reconciling a mechanical model of first- and second-order phase transitions with the magnetic counterparts, using A.C. and D.C. magnetic measurements.
Specific Heat
Low temperature measurements of sample's heat capacity is done using the
pulse and/or the ac method. The ac technique is well suited for heat capacity
measurements around phase transition temperatures. The set-up has been tested
and run on indium doped tin-lead-tellurides, semiconductor materials with
superconducting properties (in collaboration with D. I. Popov and S. A. Nemov)
and ferric Chloride intercalated graphite, a 2D electronic and magnetic system
(in collaboration with G. O. Zimmerman). The preliminary results on SnPbTe-In
show a specific heat anomaly due to superconducting transition, which has been
correlated with resistivity and susceptibility measurements. The preliminary
results on the GIC's also show a phase transition below 2 K, just like previous
results on different stage samples.
Materials and Systems of Interest
Layered materials (intercalated graphite), two dimentional magnetic and electronic systems, metal alloys and metalo-organic films, and superconductors.